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Hindered alkenes, however, may undergo hydroboration at high pressure and may even yield trialkylboranes 43 It is clear from these representative results that regioselectivity in hydroboration is controlled by steric effects. As a result, nonsymmetric internal olefins usually yield a mixture of regioisomeric alkylboranes when they react with borane. Several hindered mono- and diakylboranes with sterically demanding alkyl groups, however, have been developed for use in selective hydroboration. Disiamylborane [bis(3-methyl-2-butyl)borane, 34], thexylborane (2,3-dimethyl-2-butylborane, 35), and 9-BBN (9-borabicyclo[3.3.1]nonane) are the most frequently used reagents 37,339,342 Improvements of regioselectivities in hydroboration of both terminal and internal alkenes can be achieved with such hindered dialkylboranes 40,344 Disiamylborane shifts the selectivity to the formation of the regioisomer substituted at the less hindered olefinic carbon 40

44-83%

entire suspension is well mixed. The two agitators can be rotated cocurrently (Ekato) or countercurrently (Cellier) (Thibault, 1999). The effect of mixing (time and intensity) on the rheology of the pigment slurry is summarized by Robinson et al. (1997). Breakdown of the dispersion agglomerates requires imposition of shear on the slurry. Consequently, the impeller tip speed is critical for disperser operation and mixer design. As the maximum shear rate [ranging from 100 to 104 s 1 in dispersion operations (Makinen, 1999)] determines the ultimate size of the particles, extending the dispersion time cannot compensate for an inadequate shear level. The second step in coating preparation is the coating formulation. The dispersed pigment is mixed with appropriate binders and cobinders (adhesives, such as starches and latexes) and other additives (optical whiteners and viscosity modi ers) to achieve the properties required for the coating. The quantity of materials and their order of addition greatly in uences the ease of mixing and the properties and quality of the nal color preparation (Makinen, 1999). The order in which the coating components are added determines their interaction with each other, and consequently, the size of the pigment particles and the rheology of the slurry. Certain components, if added in a particular order, rapidly form viscous mixtures that suddenly and dramatically increase the load on the mixer, placing unacceptable loads on it. Continued mixing may reduce the overall mixture viscosity as slurry aggregates are comminuted by shear during mixing. However, the nal quality (rheology) of the color may not be an optimum. Once prepared, coating colors are kept in motion, by either mixing or recirculation, until applied to paper in a coating nip, where the shear rate can approach 106 s 1 .

Something is awry when households consist of multiple customers having the same first name. These households probably have one individual being assigned multiple CUSTOMERIDs. To investigate this, let s ask the question: How many households consist of different customers that have the same first name and the same gender

The code is only available as a checkout from the project CVS repository, so fetching it and setting it up in your development environment may or may not be worth the trouble to you your mileage may vary. So, check it out if you like setting up a local feed validator is left as an exercise for you. In any case, I cannot stress the value of having access to a validator for your feeds, and using it. It s really the only way to get a sort of independent opinion on how clean and well put-together your feeds are, and the only way feed aggregators and producers can try to follow standards and escape a tag soup mess like the haphazard HTML that has plagued Web development throughout its history. So, throughout this part of the book, you should not only check to see that your programs run without error, when they produce feeds, you should also ensure that your programs have run correctly and produce valid feeds.

You have four ways to get your artwork from FreeHand to Flash: the .SWF export feature from FreeHand, copy-and-paste, drag and drop, and now in Flash 5 you can open FreeHand 9 files directly in Flash.

The standardized form of JavaScript is called ECMAScript. This is a relevant fact because, usually, if you con ne your scripting to the conventions of the W3C s Level 1 DOM and ECMAScript, you ll be pretty successful at achieving cross-browser scripting compatibility.

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